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  1. Monatshefte für Chemie - Chemical Monthly
  2. Monatshefte für Chemie - Chemical Monthly : Volume 148
  3. Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 2, February 2017
  4. The phase transition of Pb8F14I2
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Monatshefte für Chemie - Chemical Monthly : Volume 148
Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 6, June 2017
Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 5, May 2017
Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 4, April 2017
Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 3, March 2017
Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 2, February 2017
Thanks to our Reviewers
The phase transition of Pb8F14I2
Pentaazatetraethylene supported polyacrylamide (PAA-N5) as a novel adsorbent for the efficient removal of industrial dyes from aqueous solutions: adsorption isotherms and kinetics
Interaction of TiO2 nanoparticle with trypsin analyzed by kinetic and spectroscopic methods
Solvothermal syntheses, crystal structures, and properties of new lanthanide compounds based on tetraselenidoantimonate and tetraethylenepentamine mixed ligands
Novel dyes of branched chain polymeric metal complexes with benzodithiophene or hydroquinone derivatives as donor: synthesis, characterization, and photovoltaic performance for dye-sensitized solar cells
Conformational, IR, NMR, and EPR analysis of ifosfamide by density functional theory calculation
Synthesis and study of the electronic properties of pyrazolo[1,5-c]pyrrolo[1,2-a]quinazoline and pyrazolo[1,5-c]pyrido[1,2-a]quinazoline derivatives
Electrochemical investigations of some newly synthesized arylazapyrazole derivatives
Photochemical and DNA degradation studies on tenoxicam, lornoxicam, and their photolysis products
Synthesis of new pyrido-benzodiazepine salts and their antimicrobial activities
Synthesis of novel three compound imidazole derivatives via Cu(II) catalysis and their larvicidal and antimicrobial activities
Synthesis of some new 1,2,4-triazoles containing olyl moiety and evaluation of their antimicrobial and antioxidant activities
Synthesis, antitumor evaluation, and molecular docking studies of indole–indazolyl hydrazide–hydrazone derivatives
A novel analogue of Asinger reaction for the synthesis of thiazinoquinoline derivatives
Green and recyclable sulfonated graphene and graphene oxide nanosheet catalysts for the syntheses of 3,4-dihydropyrimidinones
A green and convenient approach for the one-pot solvent-free synthesis of coumarins and β-amino carbonyl compounds using Lewis acid grafted sulfonated carbon@titania composite
Heteropolyacid catalyzed formation of thioparabanic acid derivatives
Mixed cobalt/nickel metal–organic framework, an efficient catalyst for one-pot synthesis of substituted imidazoles
Allylic oxidation of cyclic alkenes with molecular oxygen and tert-butyl hydroperoxide over copper-manganese oxides
Synthesis and characterization of supramolecule grafted on modified magnetic nanoparticles: new hybrid organic–inorganic phase transfer catalyst
One-pot multicomponent asymmetric synthesis of α-amidosulfides from thiophenol and N-acylimines generated in situ from α-amidosulfones
NaBrO3/bmim[HSO4]: a versatile system for the selective oxidation of 1,2-diols, α-hydroxyketones, and alcohols
Rapid oxidation of dibenzothiophene in model fuel under ultrasound irradiation
Monatshefte für Chemie - Chemical Monthly : Volume 148, Issue 1, January 2017
Monatshefte für Chemie - Chemical Monthly : Volume 147
Monatshefte für Chemie - Chemical Monthly : Volume 146
Monatshefte für Chemie - Chemical Monthly : Volume 145
Monatshefte für Chemie - Chemical Monthly : Volume 144
Monatshefte für Chemie - Chemical Monthly : Volume 143
Monatshefte für Chemie - Chemical Monthly : Volume 142
Monatshefte für Chemie - Chemical Monthly : Volume 141
Monatshefte für Chemie - Chemical Monthly : Volume 140
Monatshefte für Chemie - Chemical Monthly : Volume 139
Monatshefte für Chemie - Chemical Monthly : Volume 138
Monatshefte für Chemie - Chemical Monthly : Volume 137
Monatshefte für Chemie - Chemical Monthly : Volume 136
Monatshefte für Chemie - Chemical Monthly : Volume 135
Monatshefte für Chemie - Chemical Monthly : Volume 134
Monatshefte für Chemie - Chemical Monthly : Volume 133
Monatshefte für Chemie - Chemical Monthly : Volume 132
Monatshefte für Chemie - Chemical Monthly : Volume 131
Monatshefte für Chemie - Chemical Monthly : Volume 130
Monatshefte für Chemie - Chemical Monthly : Volume 129
Monatshefte für Chemie - Chemical Monthly : Volume 128

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The phase transition of Pb8F14I2

Content Provider SpringerLink
Author Weil, Matthias
Copyright Year 2016
Abstract The reversible phase transition of Pb8F14I2 is of continuous type and takes place at about 107 °C as monitored by temperature-dependent single crystal and powder X-ray diffraction measurements, optical microscopy, and differential scanning calorimetry. The low-temperature ferroelastic phase crystallizes in the orthorhombic crystal system (23 °C, Bmmb, Z = 2, a = 6.0699(6) Å, b = 6.0165(6) Å, c = 25.077(2) Å, 1487 structure factors, 41 parameter, R(F 2 ) = 0.0346, wR(F 2) = 0.0771) and changes its symmetry to the tetragonal crystal system into the high-temperature paraelastic phase (130 °C, I4/mmm, Z = 1, a = 4.2667(12) Å, c = 25.388(7) Å, 430 structure factors, 303 parameter, R(F 2 ) = 0.0575, wR(F 2) = 0.1564). Group–subgroup relationships between the two structures and a hypothetical intermediate structure are presented.
Starting Page 183
Ending Page 189
Page Count 7
File Format PDF
ISSN 00269247
Journal Monatshefte für Chemie - Chemical Monthly
Volume Number 148
Issue Number 2
e-ISSN 14344475
Language English
Publisher Springer Vienna
Publisher Date 2016-10-28
Publisher Place Vienna
Access Restriction One Nation One Subscription (ONOS)
Subject Keyword Lead fluoride halide Crystal structure determination Thermal analysis Group–subgroup relationships Chemistry/Food Science Organic Chemistry Inorganic Chemistry Analytical Chemistry Physical Chemistry Theoretical and Computational Chemistry
Content Type Text
Resource Type Article
Subject Chemistry
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